Molecules, Vol. 27, Pages 8674: Establishment of an LC-MS/MS Method for the Determination of 45 Pesticide Residues in Fruits and Vegetables from Fujian, China
Molecules, Vol. 27, Pages 8674: Establishment of an LC-MS/MS Method for the Determination of 45 Pesticide Residues in Fruits and Vegetables from Fujian, China
Molecules doi: 10.3390/molecules27248674
Authors:
Kunming Zheng
Xiaoping Wu
Jiannan Chen
Jinxing Chen
Wenhao Lian
Jianfeng Su
Lihong Shi
Pesticide residues in food have become an important factor seriously threatening human health. Therefore, this study was conducted to determine the pesticide residues in fruits and vegetables commonly found in Fujian, China, with the aim of constructing a simple and rapid method for pesticide residue monitoring. We collected 5607 samples from local markets and analyzed them for the presence of 45 pesticide residues. A fast, easy, inexpensive, effective, robust, and safe (QuEChERS) multi-residue extraction method followed by liquid chromatography equipped with triple-quadrupole mass spectrometry (LC-MS/MS) was successfully established. This 12-min-long analytical method detects and quantifies pesticide residues with acceptable validation performance parameters in terms of sensitivity, selectivity, linearity, the limit of quantification, accuracy, and precision. The linear range of the calibration curves ranged from 5 to 200 mg/L, the limits of detection for all pesticides ranged from 0.02 to 1.90 μg/kg, and the limits of quantification for the pesticides were 10 μg/kg. The recovery rates for the three levels of fortification ranged from 72.0% to...
Source: Molecules - Category: Chemistry Authors: Kunming Zheng Xiaoping Wu Jiannan Chen Jinxing Chen Wenhao Lian Jianfeng Su Lihong Shi Tags: Article Source Type: research