Synthesis and Structure of 1-Substituted Semithioglycolurils

Synthesis DOI: 10.1055/s-0040-1707391 Two methods for the synthesis of previously unavailable 1-substituted semithioglycolurils were developed. These methods consist of the cyclocondensation of 1-substituted ureas with 4,5-dihydroxy- or 4,5-dimethoxyimidazolidine-2-thione or glyoxal, followed by the reaction of the resulting 1-substituted 4,5-dihydroxyimidazolidine-2-ones with HSCN in a two-step one-pot procedure. Two of the desired semithioglycolurils were obtained as conglomerates. [...] © Georg Thieme Verlag Stuttgart · New YorkArticle in Thieme eJournals: Table of contents  |  Abstract  |  Full text

Source: Synthesis - May 24, 2020 Category: Chemistry Authors: Baranov, Vladimir V. Galochkin, Anton A. Nelyubina, Yulia V. Kravchenko, Angelina N. Makhova, Nina N. Tags: paper Source Type: research