Investigation of Factors Affecting the Rate of High-Boiling-Point Solvent Removal Using a Rotary Evaporator

Synlett DOI: 10.1055/s-0042-1751532 Factors that might affect the removal time of high-boiling-point solvents with a rotary evaporator were examined. Considering several essential factors, the optimized conditions for removing a high-boiling-point solvent are suggested. The results and discussion from this work can serve as a reference for current and future organic chemists. Finally, two examples of fast and successful dehydration reactions are given to demonstrate that the rotary evaporator can be used to conduct organic syntheses. [...] Georg Thieme Verlag KG Rüdigerstraße 14, 70469 Stuttgart, GermanyArticle in Thieme eJournals: Table of contents  |  Abstract  |  Full text

Source: Synlett - January 26, 2024 Category: Chemistry Authors: Chen, Yinzhe Wang, Weiding Zhang, Qian Tags: letter Source Type: research