Optimization of subcritical water hydrolysis of pecan wastes biomasses in a semi-continuous mode.
The objective of this work was to obtain reducing sugars from pecan biomasses by the optimization of the subcritical water hydrolysis technology in a semi-continuous mode and the physicochemical and morphological characterization of these materials, such as SEM, TGA and FT-IR analysis. Temperatures of 180, 220 and 260 °C, water/solids mass ratio of 15 and 30 g water/g biomass and total reaction time of 15 min were used. The highest reducing sugar yield was 27.1 g/100 g of biomass, obtained at 220 °C and R-15 for pecan shells. TGA, SEM and FT-IR analysis indicated the modifications of structures and compositions of biomasses in fresh and hydrolyzed samples.
PMID: 32172095 [PubMed - as supplied by publisher]
Source: Bioresource Technology - Category: Biotechnology Authors: Santos MSND, Zabot GL, Mazutti MA, Ugalde GA, Rezzadori K, Tres MV Tags: Bioresour Technol Source Type: research