Improved Indophenol Titration Method for Ascorbic Acid Using a Dropper and Electronic Balance: Enhanced Convenience and Efficiency
Shokuhin Eiseigaku Zasshi. 2024;65(1):1-6. doi: 10.3358/shokueishi.65.1.ABSTRACTThe analysis of ascorbic acid using the 2,6-dichloroindophenol (DCIP) titration method is a well-established technique, but requires the skilled handling of a burette for accurate measurements. In the present study, we propose a modified DCIP titrimetric method that replaces the burette with a dropper and employs an electronic balance to measure the titrated amount by weight. The dropper used can be flexibly selected, allowing for a wide range of drop sizes, from large to very small. This modification offers several advantages, including lower ...
Source: Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan - March 3, 2024 Category: Food Science Authors: Keizo Umegaki Mika Ito Kaori Yokotani Shizuo Yamada Source Type: research

Analytical Method for Melengestrol Acetate in Livestock Products Using LC-MS/MS
Shokuhin Eiseigaku Zasshi. 2024;65(1):15-19. doi: 10.3358/shokueishi.65.15.ABSTRACTThe present study verified that it is possible to analyze melengesterol acetate using the existing multi-residue method. Melengestrol acetate was extracted from livestock products using acidic acetonitrile acidified with acetic acid in the presence of n-hexane and anhydrous sodium sulfate. The crude extracts were cleaned up using an octadecylsilanized silica gel cartridge column. Separation by HPLC was performed using an octadecylsilanized silica gel column with linear gradient elution of 0.1 vol% formic acid and acetonitrile containing 0.1 ...
Source: Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan - March 3, 2024 Category: Food Science Authors: Takatoshi Sakai Hiroyuki Kikuchi Satoru Nemoto Hiroshi Akiyama Takaaki Taguchi Tomoaki Tsutsumi Source Type: research

Implementation and Evaluation of Risk Communication Regarding Residual Pesticides
In this study, a public seminar on risk communication methods was conducted to raise awareness and disseminate accurate knowledge about residual pesticides to consumers. Additionally, surveys on consumer awareness were conducted on the attendees before and after the seminar to evaluate its effectiveness. Responses were obtained from 84 participants. The paired t-test was used to analyze the changes in awareness before and after the seminar. The results showed significant improvements in "trust in the government" and "understanding of residual pesticides." Furthermore, step-wise multiple regression analysis was performed to...
Source: Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan - March 3, 2024 Category: Food Science Authors: Nobuyuki Wakui Koichi Inoue Mari Nunome Yoshinari Suzuki Aya Takagi Rie Ito Yusuke Iwasaki Junkichi Sugiura Hiroshi Akiyama Source Type: research

Establishment of Rapid Simultaneous Analysis Method for Plant Toxins by LC-TOF-MS
Shokuhin Eiseigaku Zasshi. 2024;65(1):7-14. doi: 10.3358/shokueishi.65.7.ABSTRACTAssuming food poisoning caused by toxic plants, an LC-TOF-MS-based method for the rapid and simultaneous analysis of 16 plant toxins was established. After adding water-methanol (1 : 9) and n-hexane, the samples were homogenized and extracted, and then subjected to centrifugal separation. Without any purification procedures, LC-TOF-MS measurements were performed, and qualitative and quantitative analyses using monoisotopic ion [M+H]+ (m/z) were conducted. The addition-recovery test using curry showed that qualitative analysis was possible unde...
Source: Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan - March 3, 2024 Category: Food Science Authors: Hideki Sato Yoshinori Kawano Shiho Tanaka Junko Tsunematsu Miki Matsunaga Yoshihiro Miyao Keiko Nakamuta Source Type: research

Improved Indophenol Titration Method for Ascorbic Acid Using a Dropper and Electronic Balance: Enhanced Convenience and Efficiency
Shokuhin Eiseigaku Zasshi. 2024;65(1):1-6. doi: 10.3358/shokueishi.65.1.ABSTRACTThe analysis of ascorbic acid using the 2,6-dichloroindophenol (DCIP) titration method is a well-established technique, but requires the skilled handling of a burette for accurate measurements. In the present study, we propose a modified DCIP titrimetric method that replaces the burette with a dropper and employs an electronic balance to measure the titrated amount by weight. The dropper used can be flexibly selected, allowing for a wide range of drop sizes, from large to very small. This modification offers several advantages, including lower ...
Source: Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan - March 3, 2024 Category: Food Science Authors: Keizo Umegaki Mika Ito Kaori Yokotani Shizuo Yamada Source Type: research

Analytical Method for Melengestrol Acetate in Livestock Products Using LC-MS/MS
Shokuhin Eiseigaku Zasshi. 2024;65(1):15-19. doi: 10.3358/shokueishi.65.15.ABSTRACTThe present study verified that it is possible to analyze melengesterol acetate using the existing multi-residue method. Melengestrol acetate was extracted from livestock products using acidic acetonitrile acidified with acetic acid in the presence of n-hexane and anhydrous sodium sulfate. The crude extracts were cleaned up using an octadecylsilanized silica gel cartridge column. Separation by HPLC was performed using an octadecylsilanized silica gel column with linear gradient elution of 0.1 vol% formic acid and acetonitrile containing 0.1 ...
Source: Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan - March 3, 2024 Category: Food Science Authors: Takatoshi Sakai Hiroyuki Kikuchi Satoru Nemoto Hiroshi Akiyama Takaaki Taguchi Tomoaki Tsutsumi Source Type: research

Implementation and Evaluation of Risk Communication Regarding Residual Pesticides
In this study, a public seminar on risk communication methods was conducted to raise awareness and disseminate accurate knowledge about residual pesticides to consumers. Additionally, surveys on consumer awareness were conducted on the attendees before and after the seminar to evaluate its effectiveness. Responses were obtained from 84 participants. The paired t-test was used to analyze the changes in awareness before and after the seminar. The results showed significant improvements in "trust in the government" and "understanding of residual pesticides." Furthermore, step-wise multiple regression analysis was performed to...
Source: Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan - March 3, 2024 Category: Food Science Authors: Nobuyuki Wakui Koichi Inoue Mari Nunome Yoshinari Suzuki Aya Takagi Rie Ito Yusuke Iwasaki Junkichi Sugiura Hiroshi Akiyama Source Type: research

Establishment of Rapid Simultaneous Analysis Method for Plant Toxins by LC-TOF-MS
Shokuhin Eiseigaku Zasshi. 2024;65(1):7-14. doi: 10.3358/shokueishi.65.7.ABSTRACTAssuming food poisoning caused by toxic plants, an LC-TOF-MS-based method for the rapid and simultaneous analysis of 16 plant toxins was established. After adding water-methanol (1 : 9) and n-hexane, the samples were homogenized and extracted, and then subjected to centrifugal separation. Without any purification procedures, LC-TOF-MS measurements were performed, and qualitative and quantitative analyses using monoisotopic ion [M+H]+ (m/z) were conducted. The addition-recovery test using curry showed that qualitative analysis was possible unde...
Source: Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan - March 3, 2024 Category: Food Science Authors: Hideki Sato Yoshinori Kawano Shiho Tanaka Junko Tsunematsu Miki Matsunaga Yoshihiro Miyao Keiko Nakamuta Source Type: research

Improved Indophenol Titration Method for Ascorbic Acid Using a Dropper and Electronic Balance: Enhanced Convenience and Efficiency
Shokuhin Eiseigaku Zasshi. 2024;65(1):1-6. doi: 10.3358/shokueishi.65.1.ABSTRACTThe analysis of ascorbic acid using the 2,6-dichloroindophenol (DCIP) titration method is a well-established technique, but requires the skilled handling of a burette for accurate measurements. In the present study, we propose a modified DCIP titrimetric method that replaces the burette with a dropper and employs an electronic balance to measure the titrated amount by weight. The dropper used can be flexibly selected, allowing for a wide range of drop sizes, from large to very small. This modification offers several advantages, including lower ...
Source: Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan - March 3, 2024 Category: Food Science Authors: Keizo Umegaki Mika Ito Kaori Yokotani Shizuo Yamada Source Type: research

Analytical Method for Melengestrol Acetate in Livestock Products Using LC-MS/MS
Shokuhin Eiseigaku Zasshi. 2024;65(1):15-19. doi: 10.3358/shokueishi.65.15.ABSTRACTThe present study verified that it is possible to analyze melengesterol acetate using the existing multi-residue method. Melengestrol acetate was extracted from livestock products using acidic acetonitrile acidified with acetic acid in the presence of n-hexane and anhydrous sodium sulfate. The crude extracts were cleaned up using an octadecylsilanized silica gel cartridge column. Separation by HPLC was performed using an octadecylsilanized silica gel column with linear gradient elution of 0.1 vol% formic acid and acetonitrile containing 0.1 ...
Source: Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan - March 3, 2024 Category: Food Science Authors: Takatoshi Sakai Hiroyuki Kikuchi Satoru Nemoto Hiroshi Akiyama Takaaki Taguchi Tomoaki Tsutsumi Source Type: research

Implementation and Evaluation of Risk Communication Regarding Residual Pesticides
In this study, a public seminar on risk communication methods was conducted to raise awareness and disseminate accurate knowledge about residual pesticides to consumers. Additionally, surveys on consumer awareness were conducted on the attendees before and after the seminar to evaluate its effectiveness. Responses were obtained from 84 participants. The paired t-test was used to analyze the changes in awareness before and after the seminar. The results showed significant improvements in "trust in the government" and "understanding of residual pesticides." Furthermore, step-wise multiple regression analysis was performed to...
Source: Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan - March 3, 2024 Category: Food Science Authors: Nobuyuki Wakui Koichi Inoue Mari Nunome Yoshinari Suzuki Aya Takagi Rie Ito Yusuke Iwasaki Junkichi Sugiura Hiroshi Akiyama Source Type: research

Establishment of Rapid Simultaneous Analysis Method for Plant Toxins by LC-TOF-MS
Shokuhin Eiseigaku Zasshi. 2024;65(1):7-14. doi: 10.3358/shokueishi.65.7.ABSTRACTAssuming food poisoning caused by toxic plants, an LC-TOF-MS-based method for the rapid and simultaneous analysis of 16 plant toxins was established. After adding water-methanol (1 : 9) and n-hexane, the samples were homogenized and extracted, and then subjected to centrifugal separation. Without any purification procedures, LC-TOF-MS measurements were performed, and qualitative and quantitative analyses using monoisotopic ion [M+H]+ (m/z) were conducted. The addition-recovery test using curry showed that qualitative analysis was possible unde...
Source: Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan - March 3, 2024 Category: Food Science Authors: Hideki Sato Yoshinori Kawano Shiho Tanaka Junko Tsunematsu Miki Matsunaga Yoshihiro Miyao Keiko Nakamuta Source Type: research

Improved Indophenol Titration Method for Ascorbic Acid Using a Dropper and Electronic Balance: Enhanced Convenience and Efficiency
Shokuhin Eiseigaku Zasshi. 2024;65(1):1-6. doi: 10.3358/shokueishi.65.1.ABSTRACTThe analysis of ascorbic acid using the 2,6-dichloroindophenol (DCIP) titration method is a well-established technique, but requires the skilled handling of a burette for accurate measurements. In the present study, we propose a modified DCIP titrimetric method that replaces the burette with a dropper and employs an electronic balance to measure the titrated amount by weight. The dropper used can be flexibly selected, allowing for a wide range of drop sizes, from large to very small. This modification offers several advantages, including lower ...
Source: Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan - March 3, 2024 Category: Food Science Authors: Keizo Umegaki Mika Ito Kaori Yokotani Shizuo Yamada Source Type: research

Analytical Method for Melengestrol Acetate in Livestock Products Using LC-MS/MS
Shokuhin Eiseigaku Zasshi. 2024;65(1):15-19. doi: 10.3358/shokueishi.65.15.ABSTRACTThe present study verified that it is possible to analyze melengesterol acetate using the existing multi-residue method. Melengestrol acetate was extracted from livestock products using acidic acetonitrile acidified with acetic acid in the presence of n-hexane and anhydrous sodium sulfate. The crude extracts were cleaned up using an octadecylsilanized silica gel cartridge column. Separation by HPLC was performed using an octadecylsilanized silica gel column with linear gradient elution of 0.1 vol% formic acid and acetonitrile containing 0.1 ...
Source: Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan - March 3, 2024 Category: Food Science Authors: Takatoshi Sakai Hiroyuki Kikuchi Satoru Nemoto Hiroshi Akiyama Takaaki Taguchi Tomoaki Tsutsumi Source Type: research

Implementation and Evaluation of Risk Communication Regarding Residual Pesticides
In this study, a public seminar on risk communication methods was conducted to raise awareness and disseminate accurate knowledge about residual pesticides to consumers. Additionally, surveys on consumer awareness were conducted on the attendees before and after the seminar to evaluate its effectiveness. Responses were obtained from 84 participants. The paired t-test was used to analyze the changes in awareness before and after the seminar. The results showed significant improvements in "trust in the government" and "understanding of residual pesticides." Furthermore, step-wise multiple regression analysis was performed to...
Source: Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan - March 3, 2024 Category: Food Science Authors: Nobuyuki Wakui Koichi Inoue Mari Nunome Yoshinari Suzuki Aya Takagi Rie Ito Yusuke Iwasaki Junkichi Sugiura Hiroshi Akiyama Source Type: research